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HCID 19974265、化合物 → N-[2-(4-(2-Carbomethoxy-1-methylethenyl) phenyl)-1-methylethyl]-2-(2-trifluoromethyl-thiazol-4-yl)morpholine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | HCID 19974265 | HCID 19974265 | — |
| 反応物 | 1-[4-(2-Carbomethoxy-1-methylethenyl)phenyl]propan-2-one | HCID 54548003 | — |
| 生成物 | N-[2-(4-(2-Carbomethoxy-1-methylethenyl) phenyl)-1-methylethyl]-2-(2-trifluoromethyl-thiazol-4-yl)morpholine | HCID 54361252 | — |
反応手順
Prepared analogously to Example 13 by reaction of 2-(2-trifluoromethyl-thiazol-4-yl)morpholine with 1-[4-(2-carbomethoxy-1-methylethenyl)phenyl]propan-2-one followed by purification of the base on a silica gel column using chloroform/ethyl acetate=19:1 as eluant.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04886814 |
| 出典データセット | uspto-grants-1989_12 |
| ORD ID | ord-62544046cf964ed58ddbc4728bd1f256 |
| 出典メモ | uspto-grants-1989_12 |