HCID 10497335, compound → HCID 14155093, compound

Participants

Reaction Steps

This material was prepared by heating 2 benzylthio-5-(2,2,2-trifluoroethoxy)-1,2,4-triazolo[1,5-a]pyrimidine in boiling ethanol. The hot mixture was filtered and the filtrate was concentrated. The crude product was recrystallized from isopropanol to yield the desired product as a solid, m.p. 115°-117° C. IR and 1H NMR spectra were in agreement with the assigned structure.

Provenance & Evidence