HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenamine, 2-chloro-5-(trifluoromethyl)- → 2,6-Dichloro-3-(trifluoromethyl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenamine, 2-chloro-5-(trifluoromethyl)- | HCID 8475 | — |
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Product | 2,6-Dichloro-3-(trifluoromethyl)aniline | HCID 13470473 | — |
Reaction Steps
This material was prepared by chlorination of 2-chloro-5-trifluoromethylaniline with N-chlorosuccinimide followed by chromatographic purification. The product was isolated as a yellow oil which was characterized by IR and 1H NMR spectroscopy and combustion analysis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04886883 |
| Source dataset | uspto-grants-1989_12 |
| ORD ID | ord-f9c02b53318d4f1e9ac145e0e7814ec2 |
| Source note | uspto-grants-1989_12 |