Benzyl Bromide → HCID 14155410, compound

HRID 477263Notes

Reaction equation

HRID 477263 reaction equation
[NH2:1][C:2]1[C:9]([Cl:10])=[CH:8][CH:7]=[CH:6][C:3]=1[CH2:4][OH:5].[CH2:11](Br)[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[CH2:11]([O:5][CH2:4][C:3]1[CH:6]=[CH:7][CH:8]=[C:9]([Cl:10])[C:2]=1[NH2:1])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

3

Reactant 2

HCID 7498Benzyl BromideHCID 14155407(2-Amino-3-chlorophenyl)methanol

Product 1

HCID 14155410HCID 14155410, compound

Procedure

This material was prepared from 2-amino-3-chlorobenzyl alcohol and benzyl bromide by the general procedure outlined in Example 98. The product was purified by Kugelrohr distillation to yield an oil, b.p. 118°-125° C. (0.1 mm). The product was characterized by IR and 1H NMR spectroscopy.

Workup

  1. distillationThe product was purified by Kugelrohr distillation
  2. customto yield an oil, b.p. 118°-125° C. (0.1 mm)

Sources & evidence

ORD record
ord-33f884f803704c0cbdd50acdd5c32a65
Source dataset
uspto-grants-1989_12
Patent number
US04886883

Reaction notes

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