HCID 19835546, compound → HCID 19835519, compound

Participants

Reaction Steps

2 g (0.0057 mol) of the 1-(2'-acetylamino-4'-nitrophenoxy)-3-succinimidopropan-2-ol obtained in the second step are heated for one hour, in a boiling water-bath, in 10 ml of hydrochloric acid (specific gravity=1.18), with stirring. After the reaction medium has been cooled, diluted and rendered alkaline, the expected product precipitates. It is filtered off, washed with water and recrystallised from ethanol. It melts at 200° C.

Provenance & Evidence