Hydrochloric Acid → HCID 19835681, compound

Participants

Reaction Steps

1.09 g of 2,6-bis(methoxymethoxy)benzylamine in 60 ml of anhydrous ethyl ether are treated with 1.92 ml of a 2.25 M solution of hydrogen chloride in anhydrous ethyl ether. A white solid precipitates which after filtering and carefully washing with anhydrous ethyl ether gives 2,6-bis(methoxymethoxy)benzylamine hydrochloride with melting point 151,5°-152° C.; the yield obtained is 95%. I.R. (KBr) 2580 cm-1 (NH3+), 1252 cm-1 (aromatic C--O), 1076 cm-1 (acetalic C--O), 773 cm-1 (phenyl).

Provenance & Evidence