Bromine → HCID 14122312, compound

Participants

Reaction Steps

A solution of 9.2 ml (0.18 mol) of bromine in 72 ml of methylene chloride is added dropwise at room temperature to a suspension of 46 g of 2-chloro-4-nitrophenylcyanothioacetamide (0.18 mol) and 30 g of sodium hydrogencarbonate (0.36 mol) in 650 ml of methylene chloride. This was followed by 2 hours of stirring at room temperature, filtering off with suction and repeated washing of the yellow residue with water.

Provenance & Evidence