HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 19872293, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 178518539 | HCID 178518539 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19872293 | HCID 19872293 | — |
Reaction Steps
A mixture of the product of stage (c) (20 g), toluene (150 ml) and acetyl chloride (12.2 ml) was heated under reflux for 5 hours. The volatile materials were removed in vacuo, and the residue was triturated with ether and filtered off. Recrystallisation from ethanol gave 19.8 g of desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04889553 |
| Source dataset | uspto-grants-1989_12 |
| ORD ID | ord-e7422cc80fb543809bd09614b2f11978 |
| Source note | uspto-grants-1989_12 |