Water → HCID 54209344, compound

HRID 477906Notes

Reaction equation

HRID 477906 reaction equation
[CH:1]1[C:6]([N+:7]([O-:9])=[O:8])=[CH:5][CH:4]=[C:3]([OH:10])[CH:2]=1.Br[CH2:12][CH:13]=[CH:14][CH2:15]Br.[C:17]([O-:20])([O-])=O.[K+].[K+].[OH2:23]>CC(C)=O>[N+:7]([C:6]1[CH:5]=[CH:4][C:3]([O:10][CH2:12][CH:13]=[CH:14][CH2:15][O:20][C:17]2[CH:2]=[CH:1][C:6]([N+:7]([O-:8])=[O:23])=[CH:5][CH:4]=2)=[CH:2][CH:1]=1)([O-:9])=[O:8]

Participants

6

Reactant 4

HCID 962WaterHCID 9804-NitrophenolHCID 11430Potassium CarbonateHCID 131802-Butene, 1,4-dibromo-

Product 1

HCID 54209344HCID 54209344, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Conditions

Temperature
60 °C

Procedure

A mixture of 5.6 g of p-nitrophenol, 4.3 g of 1,4-dibromo-2-butene, and 5,6 g of K2CO3 in 80 ml of acetone was heated at 60° C. overnight. The reaction mixture was poured into water and filtered to give, after drying, 6.8 g of product as a creamy colored solid.

Workup

  1. filtrationfiltered
  2. customto give
  3. customafter drying

Sources & evidence

ORD record
ord-a5b97041095a4c3fb5e13f605b1fc534
Source dataset
uspto-grants-1989_12
Patent number
US04889868

Reaction notes

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