Phosphorus oxychloride → HCID 15055716, compound

HRID 478062Notes

Reaction equation

HRID 478062 reaction equation
[C:1]([CH2:3][C:4]1[N:5]=[C:6](O)[C:7]2[S:13][CH2:12][CH2:11][CH2:10][C:8]=2[N:9]=1)#[N:2].P(Cl)(Cl)([Cl:17])=O>>[Cl:17][C:6]1[C:7]2[S:13][CH2:12][CH2:11][CH2:10][C:8]=2[N:9]=[C:4]([CH2:3][C:1]#[N:2])[N:5]=1

Participants

3

Reactant 2

HCID 24813Phosphorus oxychlorideHCID 178510894HCID 178510894, compound

Product 1

HCID 15055716HCID 15055716, compound

Procedure

The title compound was prepared following substantially the same procedure described in Example 1, Step B using the product from Step A and phosphorus oxychloride. This procedure gave 1.2 g of product as a brown granular solid which was used in the next step.

Sources & evidence

ORD record
ord-87d7a3ac2b6a495b846dfe6385e1ee4e
Source dataset
uspto-grants-1989_12
Patent number
US04889856

Reaction notes

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