Phosphorus oxychloride → HCID 15055719, compound

HRID 478064Notes

Reaction equation

[CH2:1]([O:8][CH2:9][C:10]1[N:11]=[C:12](O)[C:13]2[S:19][CH2:18][CH2:17][CH2:16][C:14]=2[N:15]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.P(Cl)(Cl)([Cl:23])=O>>[CH2:1]([O:8][CH2:9][C:10]1[N:11]=[C:12]([Cl:23])[C:13]2[S:19][CH2:18][CH2:17][CH2:16][C:14]=2[N:15]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

Reactant 2

HCID 24813Phosphorus oxychloride

HCID 178517844HCID 178517844, compound

Product 1

HCID 15055719HCID 15055719, compound

Procedure

The title compound was prepared following substantially the same procedure described in Example 1, Step B using the title compound from Step A hereof and phosphorus oxychloride. The procedure gave 0.8 gm of product as a brown solid which was used in Step C without further purification.

Sources & evidence

ORD record: ord-ec19b1f7fc5c4633aa2101e2c1447909
Source dataset: uspto-grants-1989_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04889856

Reaction notes

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