反应详情

A solution of 2-cyano-3-cyclohexyl-3-oxo-propionic acid ethyl ester in DMSO:water (10:1) was stirred at 120° C. for 2 hours. The reaction mixture was partitioned between ether and 1N HCl, the organic phase was dried with MgSO4 and the solvent removed under reduced pressure.

1. customThe reaction mixture was partitioned between ether and 1N HCl
2. dry with materialthe organic phase was dried with MgSO4
3. customthe solvent removed under reduced pressure