HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 11579171, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Ethyl isobutyrylacetate | HCID 81583 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 11579171 | HCID 11579171 | — |
Reaction Steps
Ethyl 4-methyl-3-oxopentanoate (2.0 g, 13 mmol) was treated with 2M ammonia in ethanol (20 mL), heated to 80 C. in a sealed tube for 16 hours and concentrated to dryness to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06642222B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-c5e9ed08b4464414a250cd03cf1e8d62 |
| Source note | uspto-grants-2003_11 |