HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 10207856, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 18001152 | HCID 18001152 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 10207856 | HCID 10207856 | — |
Reaction Steps
The title compound, MS: m/e=514.4 (M+H+), [α]58920=−25.92, [α]54620=−32.60, [α]43620=−71.06, [α]36520=−152.15 (c=0.1196, chloroform), was prepared in accordance with the general method of example 102 from (−)-(1-{4-[1-(3,5-bis-trifluoromethyl-benzoyl)-3-p-tolyl-piperidin-4-yl]-piperazin-1-yl}-2,2,2-trifluoro-ethanone and methyl iodide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06642226B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-8f248d073de2434b815cd887a2bf5ae7 |
| Source note | uspto-grants-2003_11 |