Hydroxyamine hydrochloride → 1-(4-Hydroxybutyl)-4-piperidone oxime

HRID 478528Notes

Reaction equation

[OH:1][CH2:2][CH2:3][CH2:4][CH2:5][N:6]1[CH2:11][CH2:10][C:9](=O)[CH2:8][CH2:7]1.Cl.[NH2:14][OH:15]>>[OH:1][CH2:2][CH2:3][CH2:4][CH2:5][N:6]1[CH2:11][CH2:10][C:9](=[N:14][OH:15])[CH2:8][CH2:7]1

Participants

Reactant 2

HCID 443297Hydroxyamine hydrochloride

HCID 180017351-(4-Hydroxybutyl)-4-piperidone

Product 1

HCID 180017471-(4-Hydroxybutyl)-4-piperidone oxime

Procedure

1-(4-Hydroxybutyl)-4-piperidone oxime is prepared from 1-(4-hydroxybutyl)-4-piperidone and hydroxylamine hydrochloride essentially as described above in Example 38, Scheme C, step b.

Sources & evidence

ORD record: ord-d0e696a2e3784fd19238a385ff5282ad
Source dataset: uspto-grants-2003_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06642231B2

Reaction notes

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