Hydroxyamine hydrochloride → 1-(4-Methoxybutyl)-4-piperidone oxime

HRID 478530Notes

Reaction equation

[CH3:1][O:2][CH2:3][CH2:4][CH2:5][CH2:6][N:7]1[CH2:12][CH2:11][C:10](=O)[CH2:9][CH2:8]1.Cl.[NH2:15][OH:16]>>[CH3:1][O:2][CH2:3][CH2:4][CH2:5][CH2:6][N:7]1[CH2:12][CH2:11][C:10](=[N:15][OH:16])[CH2:9][CH2:8]1

Participants

Reactant 2

HCID 443297Hydroxyamine hydrochloride

HCID 180020021-(4-Methoxybutyl)-4-piperidone

Product 1

HCID 180016781-(4-Methoxybutyl)-4-piperidone oxime

Procedure

1-(4-Methoxybutyl)-4-piperidone oxime is prepared from 1-(4-methoxybutyl)-4-piperidone and hydroxylamine hydrochloride essentially as described above in Example 38, Scheme C, step b.

Sources & evidence

ORD record: ord-03b6a559abde45069b547d902b8e7a3f
Source dataset: uspto-grants-2003_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06642231B2

Reaction notes

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