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HRID478616

反应详情

EQUATION

反应方程式

HRID 478616 的结构方程式

REACTANTS

反应物

4
结构：NC1(C(=O)O)CCCCC1
HCID1366

Cyclohexanecarboxylic acid, 1-amino-

C7H13NO2

结构：[Na+].[OH-]
HCID14798

Sodium Hydroxide

HNaO

结构：O=C(Cl)OCC1c2ccccc2-c2ccccc21
HCID34367

1-(9-Fluorenyl)methyl chloroformate

C15H11ClO2

结构：CCN(C(C)C)C(C)C
HCID81531

Diisopropylethylamine

C8H19N

PRODUCTS

生成物

1
结构：NC1(C(=O)O)CCCCC1C(=O)OCC1c2ccccc2-c2ccccc21
HCID56923993

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

结构：CO.ClCCl
溶剂HCID21226129

未命名化合物

PROCEDURE

实验过程

The title compound is prepared from 1-aminocyclohexane carboxylic acid (700 mmol), FMOC-chloride (770 mmol), Diisopropyl-ethylamine (770 mmol) and 770 ml NaOH 1N in 950 ml dioxan by conventional methods. Mp. 180-182° C.; Rf=0.21 (CH2Cl2/MeOH=95:5)