HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fumaric Acid → HCID 86589625, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fumaric Acid | HCID 444972 | — |
| Reactant | Fumarate | HCID 5460307 | — |
| Reactant | HCID 18002526 | HCID 18002526 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 86589625 | HCID 86589625 | — |
Reaction Steps
Oxidation of 8-(octahydro-inden-2-yl)-1-phenyl-1,8-diaza-spiro[4.5]decan-4-ol (mixture of diastereoisomers) according to the general method of example 20 and formation of the fumarate with fumaric acid in diethyl ether yielded the title compound, pale brown solid, m.p. 225° C. and MS: m/e=353.4 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06642247B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-499ff35c5cab4675930b69ff418b33c3 |
| Source note | uspto-grants-2003_11 |