HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69852237, compound → HCID 13979733, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69852237 | HCID 69852237 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 13979733 | HCID 13979733 | 94.2% |
Reaction Steps
A mixture of methyl 6-(pyridin-2-yl)-5-hexenoate (4.97 g, 21.0 mmol) and 10% palladium on carbon (200 mg) in methanol (100 ml) was stirred overnight under hydrogen atmosphere. The reaction mixture was filtered. Evaporation of solvent from the filtrate yielded a target product, methyl 6-(pyridin-2-yl)-hexanoate (4.1 g, 94%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06642250B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-0ea0b1a3f55b428cacc96893397c267b |
| Source note | uspto-grants-2003_11 |