HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → HCID 129689385, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | Tetrafluoroboric acid | HCID 28118 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 129689385 | HCID 129689385 | — |
Reaction Steps
To a solution of imidazole (20 mmol) in dichloromethane (30 mL) at 0° C. HBF4 (20 mmol, 3.8g of a diethyl etherate) in dichloromethane is added dropwise. The reaction mixture is diluted with diethyl ether (100 mL) to precipitate the title compound. It is then filtered, washed with ether and recrystallized from ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06642373B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-1296a4ff55a94f10909d5daab4022bdf |
| Source note | uspto-grants-2003_11 |