HuagongsheHuagongshe Chemistry Print Report · For research reference only
Epichlorohydrin → HCID 18003349, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 22392274 | HCID 22392274 | — |
| Catalyst | Tetrabutylammonium hydrogen sulfate | HCID 94433 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 18003349 | HCID 18003349 | — |
Reaction Steps
Following the procedure described in Example 7, 80 g (0.37 moles) of 1-(2-hydroxyethyl)-3,3,4,5,5-pentamethyl-piperazin-2-one are reacted with 118 g (1.28 moles) of epichlorohydrin in the presence of 13 g (38 mmoles of tetrabutylammonium hydrogen sulfate and 16.4 g (0.41 moles) of sodiumhydroxide dissolved in 41 ml of water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06642383B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-f69f1f2138ff423fa6aa282f036d3c68 |
| Source note | uspto-grants-2003_11 |