Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | Cyclopropanecarbonyl chloride | HCID 77637 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 11829501 | HCID 11829501 | 102.1% |
Reaction Steps
A solution of cyclopropanecarbonyl chloride (10.0 g) in dry tetrahydrofuran was added dropwise to a solution of imidazole (13.0 g, 2 equivalents) stirred at 0° C. After 1 hour the solid was filtered and the filtrate evaporated to give the title compound (13.3 g), NMR 1.2 (m, 2H), 1.38 (m, 2H), 2.21 (m, 1H), 7.12 (d, 1H), 7.55 (d, 1H), 8.34 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06642418B1 |
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| Source dataset | uspto-grants-2003_11 |
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| ORD ID | ord-aeb4debf6a98429a89e093bb05b5679d |
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| Source note | uspto-grants-2003_11 |
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