HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10272779, compound → HCID 18003512, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10272779 | HCID 10272779 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18003512 | HCID 18003512 | 89% |
Reaction Steps
A suspension of 100 mg of 2Z-ethoxy-3-{2-methyl-4-[2-(5-methyl-2-phenyl-oxazol-4-yl)-ethoxy]-phenyl}-acrylic acid and 26 mg of Pd/C (10%) in 2 ml of MeOH was hydrogenated at 22° C./1 bar for 2 d. The suspension was filtered, the filtrate evaporated and dried to give 89 mg (89%) of the title compound as a pale yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06642389B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-f7bfa7c2dd3d4de4848442eaadf05616 |
| Source note | uspto-grants-2003_11 |