Hydrochloric Acid → HCID 18770450, compound

Participants

Reaction Steps

Concentrated hydrochloric acid (0.025 ml; 0.30 mmol) was added to a solution of 1,1′-trimethylenedi[4-[4-(3,4,5-trimethoxyphenyl)benzoyl]hexahydro-l,4-diazepine] (46 mg; 0.060 mmol) in ethanol (5 ml) and the reaction mixture was concentrated under reduced pressure. The concentrated residue was suspended in diethyl ether and collected by filtration to obtain the title compound as a colorless crystalline powder.

Provenance & Evidence