HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 4-(4-Chlorophenyl)-2-(2-methyl-1-imidazolyl)-5-(3-(2-methylphenoxy)propyl)oxazole hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 4-(4-Chlorophenyl)-2-(2-methyl-1-imidazolyl)-5-[3-(2-methylphenoxy)propyl]oxazole | HCID 9887672 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 4-(4-Chlorophenyl)-2-(2-methyl-1-imidazolyl)-5-(3-(2-methylphenoxy)propyl)oxazole hydrochloride | HCID 23431810 | — |
Reaction Steps
To a mixture of 4-(4-chlorophenyl)-2-(2-methyl-1-imidazolyl)-5-(3-(2-methylphenoxy)propyl)oxazole (1.0 g) and acetone (10 ml) was added conc. hydrochloric acid (0.3 ml) and the mixture was stood at room temperature. The precipitated crystals were collected by filtration (0.97 g). Recrystallization from ethanol gave the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06699995B1 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-6af87043127949da8464a34377af4e45 |
| Source note | uspto-grants-2004_03 |