Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diglyme → HCID 178418794, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diglyme | HCID 8150 | — |
| 반응물 | (N-Formylhydrazino)-imino acetic acid ethyl ester | HCID 86590617 | — |
| 생성물 | HCID 178418794 | HCID 178418794 | 85% |
반응 단계
A suspension of (N-Formylhydrazino)-imino acetic acid ethyl ester (9.62 g, 60.4 mmol) in diglyme (40 ml) was refluxed for 30 minutes. After cooling, the precipitated crystal was collected by filteration and washed with hexane to give 1H-1,2,4-triazol-3-carboxylic acid ethyl ester (7.28 g). Yield: 85%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06645956B1 |
| 출처 데이터셋 | uspto-grants-2003_11 |
| ORD ID | ord-eca22cda00504afa90abc92f0f741e52 |
| 출처 메모 | uspto-grants-2003_11 |