p-Toluenesulfonic acid → HCID 18770572, compound

HRID 479543Notes

Reaction equation

HRID 479543 reaction equation
[C:1]1([C:7]2[CH:15]=[CH:14][C:10]([C:11]([NH2:13])=[O:12])=[CH:9][CH:8]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:16][C:17]([CH:20]=O)([CH3:19])[CH3:18].[NH:22]1[C:26]2[CH:27]=[CH:28][CH:29]=[CH:30][C:25]=2[N:24]=[N:23]1.C1(C)C=CC(S(O)(=O)=O)=CC=1>>[N:22]1([CH:20]([NH:13][C:11](=[O:12])[C:10]2[CH:9]=[CH:8][C:7]([C:1]3[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=3)=[CH:15][CH:14]=2)[C:17]([CH3:18])([CH3:19])[CH3:16])[C:26]2[CH:27]=[CH:28][CH:29]=[CH:30][C:25]=2[N:24]=[N:23]1

Participants

5

Reactant 4

HCID 6101p-Toluenesulfonic acidHCID 12417PivalaldehydeHCID 6025064-PhenylbenzamideHCID 178418385HCID 178418385, compound

Product 1

HCID 18770572HCID 18770572, compound

Procedure

4-Phenylbenzamide, pivaldehyde, benzotriazole, and p-toluenesulfonic acid were processed as described in Example 53A to provide the desired product.

Sources & evidence

ORD record
ord-04af26c9dc2b443b9c6688ae13d4e6e0
Source dataset
uspto-grants-2003_11
Patent number
US06645968B2

Reaction notes

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