HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Leucinol → HCID 18771581, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Leucinol | HCID 111307 | — |
| Reactant | 6-Bromopyridine-2-carbaldehyde | HCID 2757009 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18771581 | HCID 18771581 | — |
Reaction Steps
2] To 6-bromo-2-pyridinecarboxaldehyde (400 mg, 2.16 mmol) was added L-leucinol (0.42 mL, 3.24 mmol) in dry CH2Cl2 (10 mL) to give 2-[(6-bromo-pyridin-2-ylmethyl)-amino]-4-methyl-pentan-1-ol as brown solid. MS m/z: 287.6 (M+H). Calc'd for Cl2H19BrN2O: 287.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06645990B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-2ed80e4067954ddb9cb4d3a623036d94 |
| Source note | uspto-grants-2003_11 |