HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluoroaniline → (E)-4-chlorostyryl-N-4-fluorophenyl Sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluoroaniline | HCID 9731 | — |
| Reactant | (E)-2-(4-chlorophenyl)ethene-1-sulfonyl chloride | HCID 5938154 | — |
| Product | (E)-4-chlorostyryl-N-4-fluorophenyl Sulfonamide | HCID 8497205 | 68.5% |
Reaction Steps
A solution of (E)-4-chlorostyrylsulfonyl chloride (10 mmol) and 4-fluoroaniline (10 mmol) was subjected to General Procedure 1, part B. The title compound, melting point 105-107° C., was obtained in 68.5% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06646009B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-585b58fcbe8f43ef903c86a6f4442ca8 |
| Source note | uspto-grants-2003_11 |