HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfanilamide → (E)-styryl-N-4-sulfamylphenyl Sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfanilamide | HCID 5333 | — |
| Reactant | (E)-2-phenylethene-1-sulfonyl chloride | HCID 5369377 | — |
| Product | (E)-styryl-N-4-sulfamylphenyl Sulfonamide | HCID 854239 | 80% |
Reaction Steps
A solution of (E)-styrylsulfonyl chloride (10 mmol) and sulfanilamide (10 mmol) was subjected to General Procedure 1, part B. The title compound, melting point 171-173° C., was obtained in 80% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06646009B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-6e677487ef174c3c9bf2334179cb47a1 |
| Source note | uspto-grants-2003_11 |