Sodium Hydroxide → HCID 23698652, compound

Participants

Reaction Steps

A 4-necked, 1-liter flask equipped with a stirrer, a thermometer, a dropping funnel and a condenser tube was charged with 163.1 g (0.824 mole of 3,5-dichlorothiophenol) of the crude 3,5-dichlorothiophenol (purity 90.4%) prepared by the process of Example 1, and 370 g (0.925 mole) of an aqueous solution of 10 wt % sodium hydroxide. After 15 minutes of reaction at 25° C., the reaction mixture was subjected to separation procedure to give an aqueous solution of sodium 3,5-dichlorothiophenolate.

Provenance & Evidence