p-Chlorothiophenol → HCID 23693160, compound

Participants

Reaction Steps

A 4-necked, 1-liter flask equipped with a stirrer, a thermometer, a dropping funnel and a condenser tube was charged with a monochlorobenzene solution (0.871 mole of 4-chlorothiophenol) of 4-chlorothiophenol (13.3% of impurities) prepared by the process of Example 2 and 520 g (0.929 mole) of an aqueous solution of 10 wt % potassium hydroxide. The mixture was reacted at 25° C. for 15 minutes and was subjected to separation procedure to give an aqueous solution of potassium 4-chlorothiophenolate.

Provenance & Evidence