HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 18768666, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 17887112 | HCID 17887112 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18768666 | HCID 18768666 | — |
Reaction Steps
The product of example 30 is heated for 3 hours at 40° C. in a solution of CH2Cl2 containing 11 ml of CF3COOH. The solvent is evaporated off and the substance crystallised in acetone. The named product is obtained: M. P. 173-175° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06649627B1 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-d34379b090814baab78f5b9c52aafc7b |
| Source note | uspto-grants-2003_11 |