2-Bromo-6-[[(1,1-dimethylethyl)dimethylsilyl]oxy]naphthalene → 1-[6-(Tert-butyldimethylsilyloxy)-2-naphthyl]-3-methyl-1-(1-trityl-1h-imidazol-4-yl)-1-butanol

Participants

Reaction Steps

6-Bromo-2-tert-butyldimethylsilyloxynaphthalene (33.7 g) and 3-methyl-1-(1-trityl-1H-imidazol-4-yl)-1-butanone (31.5 g) were used as the starting materials. By the same procedure described in Reference example 1, the titled compound (40.6 g) was obtained as a colorless powder.

Provenance & Evidence