HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Tri-n-butylstannyl)thiophene → HCID 178450048, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Tri-n-butylstannyl)thiophene | HCID 2779373 | — |
| Reactant | 6-[1-Hydroxy-2-methyl-1-(1-trityl-1H-imidazol-4-yl)propyl]-2-naphthyl Trifluoromethanesulfonate | HCID 22285055 | — |
| Product | HCID 178450048 | HCID 178450048 | — |
Reaction Steps
In a similar manner to that described in Example 2-(i), the reaction was carried out by using 6-[1-hydroxy-2-methyl-1-(1-trityl-1H-imidazol-4-yl)propyl]-2-naphthyl trifluoromethanesulfonate (2.0 g) and 2-(tributylstannyl)thiophene (1.27 mL) to give the titled compound (1.43 g) as a colorless powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06649643B1 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-afdf471bf59e47b9993ef39dc88a56a1 |
| Source note | uspto-grants-2003_11 |