HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fumaric Acid → HCID 178458198, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fumaric Acid | HCID 444972 | — |
| Reactant | HCID 178458196 | HCID 178458196 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178458198 | HCID 178458198 | 88.7% |
Reaction Steps
To a heated (70° C.) solution of (S)-(−)-6-[1-hydroxy-1-(1H-imidazol-4-yl)propyl]-N-methyl-2-naphthamide (6.20 g) was added a hot solution of fumaric acid (2.20 g) in EtOH (30 mL), and the mixture was stand at room temperature. The obtained crystals were filtered, washed with EtOH, and dried in vacuo to give the title compound (7.15 g) as a colorless powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06649643B1 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-dbf83e93ba0a4a4cb62370b0ff8dc66a |
| Source note | uspto-grants-2003_11 |