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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 480507Generated: October 30, 2026

Fumaric Acid → HCID 178458198, compound

https://huagongshe.com/reaction/480507

Reaction equation

Participants

RoleNameHCIDCharge
ReactantFumaric AcidHCID 444972—
ReactantHCID 178458196HCID 178458196—
SolventEthanolHCID 702—
ProductHCID 178458198HCID 17845819888.7%

Reaction Steps

To a heated (70° C.) solution of (S)-(−)-6-[1-hydroxy-1-(1H-imidazol-4-yl)propyl]-N-methyl-2-naphthamide (6.20 g) was added a hot solution of fumaric acid (2.20 g) in EtOH (30 mL), and the mixture was stand at room temperature. The obtained crystals were filtered, washed with EtOH, and dried in vacuo to give the title compound (7.15 g) as a colorless powder.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06649643B1
Source datasetuspto-grants-2003_11
ORD IDord-dbf83e93ba0a4a4cb62370b0ff8dc66a
Source noteuspto-grants-2003_11