HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → HCID 86587193, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | N-Methylmaleimide | HCID 70261 | — |
| Reactant | HCID 86587194 | HCID 86587194 | — |
| Reactant | HCID 86587195 | HCID 86587195 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86587193 | HCID 86587193 | — |
Reaction Steps
To 20 mL of tetrahydrofuran was added 50 mmole of N-methylmaleimide, 10 mmole of hexafluorobutyl-5-norbornene-2-carboxylate, 40 mmole of 2,6-difluoro-1-methylbenzylacrylate and 0.3 g of AIBN, and the resulting solution was reacted at about 65° C. for about 12 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06653047B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-94a78c7e2a854180a897ba4f24b78a41 |
| Source note | uspto-grants-2003_11 |