HCID 69943756, compound → HCID 69944557, compound

Participants

Reaction Steps

To a solution of 4-(aminosulfonyl) 3-chloro 5-hydroxy 6-nitro pyridine (4.36 mmol) in ethyl acetate, was added 10% Pd/C (500 mg). The mixture was flushed with argon, and then stirred under a hydrogen atmosphere at balloon pressure for 4 hours at room temperature. The mixture was filtered through celite and the celite was washed with methanol. The solvent was evaporated to give the desired product.

Provenance & Evidence