HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosulfonic acid → HCID 18766653, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosulfonic acid | HCID 24638 | — |
| Reactant | 4-Amino-3-methoxybenzonitrile | HCID 11815931 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 18766653 | HCID 18766653 | — |
Reaction Steps
To a solution of 4-cyano-2-methoxyaniline (1 mmol) in chloroform (1 mL) at −78° C. is added chlorosulfonic acid. Upon reaction completion, the crude material is concentrated and may be purified by recrystalization to give N-(4-cyano-2-methoxyphenyl)-sulfamic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06653347B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-a8a0e5620d3d4631960543ac88b34b4c |
| Source note | uspto-grants-2003_11 |