HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromoaniline → HCID 69677023, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromoaniline | HCID 11992 | — |
| Reactant | HCID 18766652 | HCID 18766652 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 69677023 | HCID 69677023 | — |
Reaction Steps
To a solution of N-(4-cyano-2-methoxyphenyl)-sulfamoyl chloride (1 mmol) in DMF (1 mL) is added 2-bromoaniline (1 mmol). Upon completion of the reaction, an aqueous work up is performed. The crude material will be purified by either recrystalization or chromatography to give N-(4-Cyano-2-methoxyphenyl)-N′-(2-bromophenyl) sulfamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06653347B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-8fc27b3828b24c76b31f95b5b8ba0beb |
| Source note | uspto-grants-2003_11 |