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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 481259Generated: October 31, 2026

HCID 131724224, compound → HCID 69973074, compound

https://huagongshe.com/reaction/481259

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 131724224HCID 131724224—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 69973074HCID 69973074100%

Reaction Steps

To a solution of 117f (293 mg, 0.337 mmol) in 5 mL MeOH, was added 29 mg 10% Pd-C. The mixture was evacuated and flushed with H2 (3×), then was stirred under an atmosphere of H2 for 45 min. The mixture was filtered and concentrated in vacuo to afford 217 mg (100%) of 117g as a colorless glass. MS(ESI) 645.4 (M+H+)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06653295B2
Source datasetuspto-grants-2003_11
ORD IDord-24cd192f84c94caeaa45d71a6e52230c
Source noteuspto-grants-2003_11