HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131724224, compound → HCID 69973074, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131724224 | HCID 131724224 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 69973074 | HCID 69973074 | 100% |
Reaction Steps
To a solution of 117f (293 mg, 0.337 mmol) in 5 mL MeOH, was added 29 mg 10% Pd-C. The mixture was evacuated and flushed with H2 (3×), then was stirred under an atmosphere of H2 for 45 min. The mixture was filtered and concentrated in vacuo to afford 217 mg (100%) of 117g as a colorless glass. MS(ESI) 645.4 (M+H+)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06653295B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-24cd192f84c94caeaa45d71a6e52230c |
| Source note | uspto-grants-2003_11 |