HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 67680790, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Norchlorcyclizine | HCID 9340 | — |
| Reactant | 4-(Bromomethyl)phenylacetic acid | HCID 4519056 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 67680790 | HCID 67680790 | — |
Reaction Steps
Using 2.4 g of 4-bromomethylphenylacetic acid, 2.9 g of 1-[(4-chlorophenyl)phenylmethyl]piperazine, 2.8 ml of triethylamine, and 100 ml of dioxane, the reaction procedure of Example 1 was otherwise repeated and recrystallized from benzene-hexane to provide 1.8 g of methyl 4-[[4-[(4-chlorophenyl)phenylmethyl]-1-piperazinyl]methyl]phenylacetate melting at 113° C.-115° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05789409 |
| Source dataset | uspto-grants-1998_08 |
| ORD ID | ord-cb5d0562268f4f3585c07e0fc5cdeb6c |
| Source note | uspto-grants-1998_08 |