HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 19066218, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 1-(2-Fluorophenyl)piperazine | HCID 70529 | — |
| Reactant | Triphosgene | HCID 94429 | — |
| Reactant | HCID 19066233 | HCID 19066233 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19066218 | HCID 19066218 | 88% |
Reaction Steps
Compound 41A is prepared according to the procedure described for compound 15A, using the following reactants: 1-(2-fluorophenyl)piperazine (1.54 g, 8.06 mmol); triphosgene (850 mg, 2.85 mmol); pyridine (0.69 ml, 8.6 mmol); dichloromethane (60 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05789412 |
| Source dataset | uspto-grants-1998_08 |
| ORD ID | ord-3a4bf673753c44abb160ff17a10aff90 |
| Source note | uspto-grants-1998_08 |