HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetyl chloride → HCID 19066159, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-(2,3-Dimethoxyphenyl)piperazine | HCID 18669088 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 19066159 | HCID 19066159 | 98% |
Reaction Steps
Compound 50A is prepared according to the procedure described for compound 12, using the following reactants: chloroacetyl chloride (150 ml, 1.87 mmol); 1-(2,3-dimethoxyphenyl)piperazine (29A) (416 mg, 1.87 mmol); potassium carbonate (645 mg, 4.67 mmol); methyl ethyl ketone (20 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05789412 |
| Source dataset | uspto-grants-1998_08 |
| ORD ID | ord-b4de8338dec94f2fa2a54cbc171fefa7 |
| Source note | uspto-grants-1998_08 |