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HRID481545

反应详情

EQUATION

反应方程式

HRID 481545 的结构方程式

REACTANTS

反应物

2
结构：CO.Cl
HCID21893726

Hydrochloride methanol

CH5ClO

结构：COc1ccc(C(C)(C)C2SCCS2)cc1CN[C@H]1CCCN(C(=O)OC(C)(C)C)[C@H]1c1ccccc1
HCID86752973

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(C(C)(C)C2SCCS2)cc1CN[C@H]1CCCN[C@H]1c1ccccc1.Cl.Cl
HCID86752974

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

To a solution of Compound 82 (0.128 g) in EtOAc (5 ml) was added an excess amount of 10% HCl-MeOH (1 ml) for 8 hr. The resulting precipitate was collected and washed with EtOAc to give Compound 83 (0.069 g) as a colorless crystal.

WORKUP

后处理

  1. customThe resulting precipitate was collected
  2. washwashed with EtOAc