HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19065568, compound → HCID 19065571, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19065568 | HCID 19065568 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 19065571 | HCID 19065571 | — |
Reaction Steps
A solution of 1-[3-(4-fluorophenoxy)phenyl]-1,4-pentanedione (19.03 g; 0.0665M) in 0.44M aqueous NaOH solution (300 ml) was refluxed for 24 hrs. After cooling, the residual solids were collected by filtration and dried to give 18 g (yield quant.) of the subtitle compound [D] as brown solids, which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05792882 |
| Source dataset | uspto-grants-1998_08 |
| ORD ID | ord-84f5ff03857d401894cec7c07f5019ad |
| Source note | uspto-grants-1998_08 |