Chlorine → HCID 19063429, compound

Participants

Reaction Steps

SO2Cl2 (1.17 g, 8.65 mmol) was added to O-nonylcarbonyloxymethyl S-ethyl carbonothioate (Example 1ad(ii), 2.10 g, 7.22 mmol) in CH2 Cl2 (5 ml) at 0° C. with stirring during 15 min. followed by stirring at ambient temperature for 17 hours. Evaporation of EtSCl at 30° C. and 20 mmHg gave a yellow liquid.

Provenance & Evidence