Aniline → HCID 131720804, compound

HRID 482488Notes

Reaction equation

HRID 482488 reaction equation
[ClH:1].[NH2:2][C:3]1[C:12]2[C:7](=[CH:8][C:9]([O:15][CH3:16])=[C:10]([O:13][CH3:14])[CH:11]=2)[N:6]=[C:5]([N:17]2[CH2:22][CH2:21][N:20]([C:23](=[O:30])[CH2:24][C:25](OCC)=[O:26])[CH2:19][CH2:18]2)[N:4]=1.[NH2:31][C:32]1[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=1>CN(C=O)C>[OH2:13].[ClH:1].[NH2:2][C:3]1[C:12]2[C:7](=[CH:8][C:9]([O:15][CH3:16])=[C:10]([O:13][CH3:14])[CH:11]=2)[N:6]=[C:5]([N:17]2[CH2:18][CH2:19][N:20]([C:23](=[O:30])[CH2:24][C:25]([NH:31][C:32]3[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=3)=[O:26])[CH2:21][CH2:22]2)[N:4]=1.[NH2:2][C:3]1[C:12]2[C:7](=[CH:8][C:9]([O:15][CH3:16])=[C:10]([O:13][CH3:14])[CH:11]=2)[N:6]=[C:5]([N:17]2[CH2:18][CH2:19][N:20]([C:23](=[O:30])[CH2:24][C:25]([NH:31][C:32]3[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=3)=[O:26])[CH2:21][CH2:22]2)[N:4]=1.[ClH:1]

Participants

4

Reactant 2

HCID 6115AnilineHCID 19063096HCID 19063096, compound

Product 1

HCID 131720804HCID 131720804, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Conditions

Temperature
155 °C

Procedure

A mixture of 4 g of the compound obtained in Example 18 and 14 ml aniline in 6 ml DMF is warmed at 155° C. for 5.5 h.

Sources & evidence

ORD record
ord-8e97871a4fad42e0b428304a18a84d05
Source dataset
uspto-grants-1998_08
Patent number
US05798362

Reaction notes

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