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HRID482578

反应详情

EQUATION

反应方程式

HRID 482578 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)N
HCID6385

tert-Butylamine

C4H11N

结构：COC(=O)c1c(O)c2ccccc2[nH]c1=O
HCID54676766

Methyl 1,2-dihydro-4-hydroxy-2-oxo-3-quinolinecarboxylate

C11H9NO4

PRODUCTS

生成物

1
结构：CC(C)(C)NC(=O)c1c(O)c2ccccc2[nH]c1=O
HCID54713534

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

8.76 g (0.04 mol) of methyl 4-hydroxy-2-oxoquinoline-3-carboxylate was stirred with 3.7 g (0.05 mol) of tert-butylamine in 60 ml of ethanol in a miniautoclave for 8 hours at 150° C. under autogenous pressure. After cooling, the crystals were removed by suction filtration, washed with ligroin and dried.

WORKUP

后处理

  1. temperatureAfter cooling
  2. customthe crystals were removed by suction filtration
  3. washwashed with ligroin
  4. customdried