HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Ethanedithiol → 2-(4-Methoxyphenyl)-1,3-dithiolane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Ethanedithiol | HCID 10902 | — |
| Reactant | 4-Methoxybenzaldehyde | HCID 31244 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | 2-(4-Methoxyphenyl)-1,3-dithiolane | HCID 23175 | 99.5% |
Reaction Steps
Following the general procedure as in Example 1, 25 gm (0.184 moles) of 4-methoxybenzaldehyde and 17.3 gm (0.184 moles) of 1,2-ethanedithiol gave, after crystallization from hexane, 39.3 gm (0.183 moles) of a white colored solid (96% yield) m.p. 62°-63° C. Elemental analysis for C10H12OS2 :
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04575565 |
| Source dataset | uspto-grants-1986_03 |
| ORD ID | ord-fac1300a410d435390d745fc79f7633a |
| Source note | uspto-grants-1986_03 |